Реакция #1106665

Уравнение реакции

1,8-dichloroanthraquinone

N,N-dimethylethylenediamine

→

Compound 6

1,8-bis(2-(dimethylamino)ethylamino)anthracene-9,10-dione

Растворители

water

Условия реакции

Обработка

1. 1
   Температураwas refluxed for 18 h
2. 2
   Другоеto precipitate the title compound which
3. 3
   Другоеwas recrystallised from methanol

Методика

A mixture of 1,8-dichloroanthraquinone (5.5 g, 20 mmol) and N,N-dimethylethylenediamine (40 mL) was refluxed for 18 h. The mixture was cooled to room temperature and diluted with water to precipitate the title compound which was recrystallised from methanol to afford Compound 6 (4.5 g). The structure of Compound 6 is given below:

Источник