Реакция #1095849

Уравнение реакции

Urocanic acid

urocanic acid

→

3-(1H-Imidazol-4-yl)propionic acid

Растворители

MeOH

Условия реакции

Обработка

1. 1
   Фильтрацияfiltered
2. 2
   Концентрированиеthe filtrate was concentrated under a reduced pressure
3. 3
   Другоеto give the objective product

Методика

Urocanic acid (3-(1H-imidazol-4-yl)-acrylic acid) (138 mg, 1 mmol) was placed in a round-bottom flask and dist MeOH was added thereto until urocanic acid was completely dissolved. To this solution, 10% Pd/C (30 mg) was added, replaced with H2 and stirred. After five hours, the loss of raw materials was confirmed, filtered, and the filtrate was concentrated under a reduced pressure to give the objective product.

Источник