Реакция #1090307

Уравнение реакции

title compounds

2-methyl-1-naphthalenol methylcarbonate

2-methyl-1-naphthol

1-naphthol

phenyl trifluoroacetate

dry ice

2-methyl-1-naphthol

2-methyl-1-naphthol

→

2-methyl-1-naphthalenol propionate

Условия реакции

Обработка

1. 1
   Другоеwere stored at room temperature

Методика

To demonstrate the storage stability of the compounds of the present invention, test samples of the title compounds of Examples 1, 2, 3, 4, 5 and 6 were placed in clear glass vials and kept on top of a laboratory desk for the time indicated. Samples of 2-methyl-1-naphthol, 1-naphthol and phenyl trifluoroacetate used as controls were similarly kept. One sample of 2-methyl-1-naphthol was stored under nitrogen and in a dry ice chest (temperature of approximately -50° C). A second sample of 2-methyl-1-naphthol and the remaining test'samples were stored at room temperature.

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