Реакция #1073160

ord-9294e126bd8b47b9b7be998f2dfcd389

Уравнение реакции

CCCCCCCCCCCCN
dodecylamine
Cl.N[C@H]1C(O)O[C@H](CO)[C@@H](O)[C@@H]1O
glucosamine hydrochloride
→
CCCCCCCCCCCCNC1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1N.Cl
N-Dodecyl-N-(2-amino-2-deoxy-glucopyranosyl)-amine hydrochloride

Реактанты

CCCCCCCCCCCCN
dodecylamine
Cl.N[C@H]1C(O)O[C@H](CO)[C@@H](O)[C@@H]1O
glucosamine hydrochloride

Реагенты

Нет

Условия реакции

Подробные условия
See reaction.notes.procedure_details.

Обработка

  1. 1
    workup.ADDITIONwere added
  2. 2
    Другоеthe product precipitated
  3. 3
    ЭкстракцияThe solid was extracted three times
  4. 4
    workup.STIRRINGby stirring with ether
  5. 5
    Фильтрацияfiltered off with suction
  6. 6
    Другоеdried under a high vacuum

Методика

46 g of dodecylamine were melted at 60° and 31 g of glucosamine hydrochloride were added, with stirring. After cooling to room temperature, the product precipitated. The solid was extracted three times by stirring with ether and filtered off with suction and then dried under a high vacuum.

Источник

DOI: 10.6084/m9.figshare.5104873.v1Патент: US04710491uspto-grants-1987_12