반응 #994
ord-d2aea31453084c8dba037f866c0833b5
반응 방정식
2-Methoxy-cinnamylalcohol
thionylchloride
piperazine
→
salt
N,N'-bis-((E)-3-(2-methoxyphenyl)-2-propenyl)piperazine
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타as described in Preparation Example 2
실험 절차
2-Methoxy-cinnamylalcohol (1.44 g) was chlorinated using thionylchloride. Subsequently, reaction with piperazine and other treatments were performed as described in Preparation Example 2, to thereby obtain 314 mg of a salt as colorless prisms.