반응 #992696

반응 방정식

Mucobromic acid

Aminoguanidine bicarbonate

carbon dioxide

→

Aminoguanidinium Mucobromate

용매

water

반응 조건

후처리

1. 1
   기타The water was removed in vacuo
2. 2
   온도with heating to approximately 90° C
3. 3
   기타The product was isolated as an off-white solid

실험 절차

Mucobromic acid (2.0 g, 7.76 mmol) was dissolved in 10 ml of distilled water. Aminoguanidine bicarbonate (1.06 g, 7.76 mmol) was added in portions at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 18 hours. The water was removed in vacuo with heating to approximately 90° C. The product was isolated as an off-white solid.

출처