반응 #992684

반응 방정식

3-Amino-1,2,4-triazole

Trifluoroacetic acid

→

3-Amino-1,2,4-Triazolium TFA

용매

water

반응 조건

후처리

1. 1
   기타The water was removed in vacuo
2. 2
   온도with heating to approximately 90° C. for 4 hours

실험 절차

3-Amino-1,2,4-triazole (1.27 g, 15.14 mmol) was dissolved in 5 ml of distilled water. Trifluoroacetic acid (1.12 ml, 15.14 mmol) was added via syringe at room temperature and the reaction was stirred at room temperature for 1 hour. The water was removed in vacuo with heating to approximately 90° C. for 4 hours.

출처