반응 #992683

반응 방정식

1,2,4-Triazole

Trifluoroacetic acid

→

1,2,4-Triazolium TFA

용매

water

반응 조건

후처리

1. 1
   기타The water was removed in vacuo
2. 2
   온도with heating to approximately 90° C. for 4 hours

실험 절차

1,2,4-Triazole (2.0 g, 28.96 mmol) was dissolved in 5 ml of distilled water. Trifluoroacetic acid (2.15 ml, 3.30 g, 28.96 mmol) was added via syringe at room temperature and the reaction was stirred at room temperature for 1 hour. The water was removed in vacuo with heating to approximately 90° C. for 4 hours.

출처