반응 #992679

반응 방정식

Hydrazine monohydrate

Trifluoroacetic acid

→

Hydrazinium TFA

용매

water

반응 조건

후처리

1. 1
   workup.STIRRINGthe reaction was stirred at room temperature overnight
2. 2
   기타The water was removed in vacuo
3. 3
   온도with heating to 80° C.
4. 4
   기타yielding product as a colorless liquid

실험 절차

Hydrazine monohydrate (4.41 ml, 90.9 mmol) was added via syringe to a 250-ml round-bottom flask containing 50 ml of distilled water with stirring at room temperature. Trifluoroacetic acid (7.0 ml, 90.9 mmol) was added via syringe and the reaction was stirred at room temperature overnight. The water was removed in vacuo with heating to 80° C., yielding product as a colorless liquid.

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