반응 #987822

반응 방정식

PGMEA

methacrylate

t-butylacrylate

acrylic acid

AIBN

→

methacrylate t-butylacrylate acrylic acid

수율 80.0%

반응 조건

후처리

1. 1
   기타The prepared solution was reacted at 66° C. for 8 hours
2. 2
   기타After the reaction
3. 3
   기타the resulting mixture was precipitated in ethyl ether
4. 4
   여과filtered
5. 5
   기타dried under vacuum condition

실험 절차

To 50 g of PGMEA were added 6 g of 9-anthracenemethyl methacrylate, 3 g of t-butylacrylate, 1 g of acrylic acid and 0.8 g of AIBN. The prepared solution was reacted at 66° C. for 8 hours. After the reaction, the resulting mixture was precipitated in ethyl ether, filtered, and dried under vacuum condition thereby obtaining poly(9-anthracenemethyl methacrylate/t-butylacrylate/acrylic acid) having a molecular weight of 11,200 (yield: 80%) (see the NMR spectrum of FIG. 2).

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