반응 #9847

ord-25be29cbfe4341219e0e5c16fc46daa6

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

A mixture of 0.276 g of toluene, 0.005 g of hexahydro-1,3,5-trihydroxy-1,3,5-triazine-2,4,6-trione (1% by mole relative to toluene), 5 g of acetic acid and 0.004 g of cobalt(II) acetate.4H2O was stirred at 60° C. in an atmosphere of oxygene gas (1 atm=0.1 MPa) for 6 hours. The resulting product in the reaction mixture was analyzed by gas chromatography and was found to yield benzoic acid and benzaldehyde in 49% and 3% yields, respectively, at 53% conversion of toluene.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07091342B2uspto-grants-2006_08