반응 #96172
ord-bb8737df082d429b8775616499e8e7ff
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1여과the solution filtered on a millepore
- 2여과filter
- 3기타to remove elemental palladium
- 4기타The solution was then evaporated
실험 절차
Bis-(dibenzylidene acetone) palladium (0.10 g; 0.17 mmole) was dissolved in methylene chloride (100 ml), and the solution filtered on a millepore filter to remove elemental palladium. Dibenzylidene acetone (0.51 mmole) was added to the solution, and the solution was stirred for 24 hours at ambient temperature. The solution was then evaporated to yield purple crystals of the tris-(dibenzylidene acetone) palladium product.