반응 #96069

반응 방정식

hydantoin

capric N-chloramide

sarcosine

sodium hydroxide

→

1-methyl-3-n-nonyl hydantoin

수율 90.0%

용매

tertiary butanol

water

반응 조건

후처리

1. 1
   추출was extracted with ether
2. 2
   기타The ether was removed by distillation

실험 절차

In accordance with the procedure described in Example 6, 41 g (0.2 mol) capric N-chloramide were reacted with sarcosine, sodium hydroxide in a mixture of tertiary butanol and water and then processed. The hydantoin remained in the aqueous solution was an oil, that was extracted with ether. The ether was removed by distillation to yield 43 g (90% yield) 1-methyl-3-n-nonyl hydantoin of the formula ##STR10## having the following analysis:

출처