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2-bromo-2'-chloro-5'-dimethylsulfamoyl-acetophenone

2-bromo-3'-chloro-5'-dimethylsulfamoyl-acetophenone

2-bromo-2'-chloro-5'-methylsulfamoyl-acetophenone

2-bromo-2'-chloro-5'-sulfamoylacetophenone

2-bromo-3'-methyl-5'-dimethylsulfamoylacetophenone

2-bromo-2'-methyl-5'-sulfamoylacetophenone

2,2'-dibromo-5'-dimethylsulfamoyl-acetophenone

2-bromo-2'-methyl-5'-dimethylsulfamoylacetophenone

→

2-bromo-3'-methyl-5'-sulfamoylacetophenone

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후처리

1. 1
   기타below were prepared in an analogous manner

실험 절차

The bromoacetophenones listed below were prepared in an analogous manner: 2,2'-dibromo-5'-dimethylsulfamoyl-acetophenone, melting point 88° C., 2-bromo-3'-chloro-5'-dimethylsulfamoyl-acetophenone, melting point 77°-78° C., 2-bromo-2'-chloro-5'-methylsulfamoyl-acetophenone, melting point 99°-101° C., 2-bromo-2'-chloro-5'-dimethylsulfamoyl-acetophenone, melting point 87°-88° C., 2-bromo-2'-chloro-5'-sulfamoylacetophenone, melting point 152°-154° C., 2-bromo-3'-methyl-5'-dimethylsulfamoylacetophenone, melting point 71°-75° C., 2-bromo-2'-methyl-5'-dimethylsulfamoylacetophenone, melting point 69°-71° C. and 2-bromo-2'-methyl-5'-sulfamoylacetophenone, melting point 112°-115° C.

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