반응 #96051

반응 방정식

2-(5-chloro-2,4-dimethoxyphenyl-imino)-4-(4-chloro-3-dipropylsulfamoylphenyl)-3-methylthiazolidin-4-ol hydrobromide

→

2-(5-Chloro-2,4-dimethoxyphenyl-imino)-4-(4-chloro-3-dipropylsulfamoylphenyl)-3-methyl-4-thiazoline hydrobromide

용매

acetic acid

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후처리

1. 1
   기타Obtained by a procedure analogous to
2. 2
   workup.DISTILLATIONafter distilling off the solvent

실험 절차

Obtained by a procedure analogous to that indicated in Example 1(b), from 2-(5-chloro-2,4-dimethoxyphenyl-imino)-4-(4-chloro-3-dipropylsulfamoylphenyl)-3-methylthiazolidin-4-ol hydrobromide, by boiling in glacial acetic acid and stirring the residue under water after distilling off the solvent. Amorphous, glassy solid; melting point 130°-150° C.

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