반응 #96042

ord-8782247c338a48c8ba5cebaf3406a2ac

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타Obtained by a procedure analogous to
  2. 2
    기타precipitating with diisopropyl ether

실험 절차

Obtained by a procedure analogous to that indicated in Example 1(b), from 4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-2-(3,4,5-trimethoxyphenyl-imino)-thiazolidin-4-ol hydrobromide, by boiling for 30 minutes in glacial acetic acid and precipitating with diisopropyl ether. Melting point 246° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04346088uspto-grants-1982_08