반응 #96040

반응 방정식

2-(3-chloro-2-methylphenyl-imino)-4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-4-thiazoline hydrobromide

ammonia

→

2-(3-Chloro-2-methylphenyl-imino)-4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-4-thiazoline

용매

triethylamine

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후처리

1. 1
   기타Obtained by a procedure analogous to

실험 절차

Obtained by a procedure analogous to that indicated in Example 2 (a), from 2-(3-chloro-2-methylphenyl-imino)-4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-4-thiazoline hydrobromide, the reaction mixture being rendered alkaline with a 20% methanolic ammonia solution instead of with triethylamine and worked up as in Example 2 (a). Colorless crystals; melting point 144°-146° C.

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