반응 #95983
ord-cb95fc6af34c400ca342213058857f0a
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타The bottle was sealed
- 2온도The bottle was then heated at 50 degrees Centigrade in a water bath for 18 hours
- 3기타The bottle was then removed from the water bath
- 4기타the polymer isolated by extraction with methanol
- 5기타to precipitate polymer
- 6기타The polymer was then dried under vacuum
실험 절차
The copolymer of allyl methacrylate and methacrylate was prepared by placing 5 grams of allyl methacrylate, 95 grams of methyl methacrylate, 300 milliliters of methylene chloride, and 1.0 gram of isopropyl peroxydicarbonate in a 28 ounce round bottle. The bottle was sealed. The bottle was then heated at 50 degrees Centigrade in a water bath for 18 hours. The bottle was then removed from the water bath, and the polymer isolated by extraction with methanol to precipitate polymer. The polymer was then dried under vacuum. Thereafter, the molecular weight was determined by inherent viscosity in methylene chloride versus poly(methyl methacrylate), and was found to be in excess of 500,000.