반응 #95958

반응 방정식

N-(9-octadecenyl)ethylenediamine

butyl 3-formylpropionate

→

4-(9-octadecenyl)-2,3,6,7-tetrahydro-1,4-diazocin-5-one

반응 조건

후처리

1. 1
   workup.DISTILLATIONAt 150° C. and under a reduced pressure of 50 mmHg, 18 g of water and 74 g of butanol were distilled off

실험 절차

Into an apparatus similar to that in Example 1, were charged 310.1 g (1 mole) of N-(9-octadecenyl)ethylenediamine and 158.2 g (1 mole) of butyl 3-formylpropionate. At 150° C. and under a reduced pressure of 50 mmHg, 18 g of water and 74 g of butanol were distilled off to obtain 4-(9-octadecenyl)-2,3,6,7-tetrahydro-1,4-diazocin-5-one.

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