반응 #95949

반응 방정식

N-(2-hydroxy)tetradecyldiethylenetriamine

butyl acetoacetate

→

4-(2-hydroxytetradecyl)aminoethyl-7-methyl-3,6-dihydro-2H-1,4-diazepin-5-one

반응 조건

후처리

1. 1
   workup.DISTILLATIONAt 150° to 160° C. and under a reduced pressure of 50 mmHg, 18 g of water and 74 g of butanol were distilled off

실험 절차

Into an apparatus similar to that in Example 1, were charged 313.5 g (1 mole) of N-(2-hydroxy)tetradecyldiethylenetriamine and 158.1 g (1 mole) of butyl acetoacetate. At 150° to 160° C. and under a reduced pressure of 50 mmHg, 18 g of water and 74 g of butanol were distilled off to obtain 4-(2-hydroxytetradecyl)aminoethyl-7-methyl-3,6-dihydro-2H-1,4-diazepin-5-one.

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