반응 #955946

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Triphenyleno[1,12-bcd]thiophene

Br2

→

7-bromotriphenyleno[1,12-bcd]thiophene

용매

chloroform

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후처리

1. 1
   여과the mixture was filtered through a Celite plug
2. 2
   세척washed by CH2Cl2
3. 3
   농축The combined filtrate was concentrated

실험 절차

Triphenyleno[1,12-bcd]thiophene (1.5 g, 5.8 mmol) was dissolved in 100 mL of chloroform. Br2 was slowly added into the reaction solution. After the reaction was stirred at room temperature for 3 days, the mixture was filtered through a Celite plug and washed by CH2Cl2. The combined filtrate was concentrated to get 2.2 g of 7-bromotriphenyleno[1,12-bcd]thiophene which was used for next step without further purification.

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