반응 #955933

반응 방정식

methyl 2,4-dimethylbenzoate

hydrazine

→

2,4-dimethylbenzohydrazide

용매

MeOH

반응 조건

후처리

1. 1
   온도the mixture was heated
2. 2
   온도under reflux for 40 hours
3. 3
   기타Then the mixture was evaporated
4. 4
   기타dried under vacuum

실험 절차

To a solution of methyl 2,4-dimethylbenzoate (2 g, 12.2 mmol) in MeOH (10 mL) was added anhydrous hydrazine (1.95 mL, 61 mmol) and the mixture was heated under reflux for 40 hours. Then the mixture was evaporated and dried under vacuum to give 2,4-dimethylbenzohydrazide as a white solid (2 g, 100%; MS (M+H, 165).

출처