반응 #955906

반응 방정식

hydrazine monohydrate

3-(1′-acryloyloxyoctadecyloxy)-4,5-dioctadecyloxy nitrobenzene

→

3-(1′-acryloyloxyoctadecyloxy)-4,5-dioctadecyloxy aniline

수율 71.4%

용매

ethanol

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후처리

1. 1
   온도via heat-refluxing for 24 hours
2. 2
   기타Via recrystallized
3. 3
   workup.ADDITIONfrom mix solution of chloroform-methanol

실험 절차

Thereafter, loaded were 3 ml of hydrazine monohydrate and 10 ml of ethanol in the presence of graphite, 3.9 g of 3-(1′-acryloyloxyoctadecyloxy)-4,5-dioctadecyloxy nitrobenzene was reduced via heat-refluxing for 24 hours. Via recrystallized from mix solution of chloroform-methanol to obtain 2.7 g of 3-(1′-acryloyloxyoctadecyloxy)-4,5-dioctadecyloxy aniline (yield: 71%).

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