반응 #95323

반응 방정식

product

2-isopropyl-2-p-chlorophenyl-acetic acid

thionyl chloride

→

2-isopropyl-2-p-chlorophenyl acetyl chloride

용매

반응 조건

후처리

1. 1
   온도the mixture was refluxed for 4 hours
2. 2
   온도was then cooled
3. 3
   기타The mixture was evaporated to dryness

실험 절차

10 g of the product of Step D were added to a mixture of 50 ml of petroleum ether (b.p.=35°-70° C.) and 20 ml of thionyl chloride and the mixture was refluxed for 4 hours and was then cooled. The mixture was evaporated to dryness to obtain 10.8 g of D 2-isopropyl-2-p-chlorophenyl acetyl chloride.

출처