반응 #95317

반응 방정식

ethyl 3,3-dimethyl-5-phenylthiopentanoate

1-chloro-2,5-pyrrolidinedione

→

ethyl 5-chloro-3,3-dimethyl-5-phenylthiopentanoate

용매

carbon tetrachloride

반응 조건

후처리

1. 1
   여과The mixture was filtered
2. 2
   농축the filtrate concentrated

실험 절차

To a solution of 1.06 g (3.09 mmol) of ethyl 3,3-dimethyl-5-phenylthiopentanoate in 10 ml of carbon tetrachloride was added 590 mg (4.4 mmol) of 1-chloro-2,5-pyrrolidinedione, and the mixture was stirred at room temperature for 2 hours. The mixture was filtered, and the filtrate concentrated to give ethyl 5-chloro-3,3-dimethyl-5-phenylthiopentanoate as an oil.

출처