반응 #951511
ord-e4be45eaf8604950a34e32fb6ac79133
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1온도the mixture is refluxed for hour
- 2농축After concentrating
실험 절차
To 2-methyl-3,4,6-trifluorobenzoic acid (3.2 g) is added thiony chloride (7 ml) and the mixture is refluxed for hour. After concentrating, 2-methyl-3,4,6-trifluorobenzoyl chloride (3.3 g) is obtained.