반응 #951511

ord-e4be45eaf8604950a34e32fb6ac79133

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    온도the mixture is refluxed for hour
  2. 2
    농축After concentrating

실험 절차

To 2-methyl-3,4,6-trifluorobenzoic acid (3.2 g) is added thiony chloride (7 ml) and the mixture is refluxed for hour. After concentrating, 2-methyl-3,4,6-trifluorobenzoyl chloride (3.3 g) is obtained.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05563138uspto-grants-1996_10