반응 #94974
ord-1e111c1e7f234f0e83ad390347bfb66e
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타at a temperature of 80° C
- 2기타was removed by this technique
실험 절차
In still another approach, an admixture of BF3 /methanol/methyl isobutyrate in a molar ratio of 1:1:0.5 was introduced to the top of a countercurrent stripping column while nitrogen was passed through the bottom of the column under atmospheric pressure at a temperature of 80° C. The effort to preferentially strip the BF3 was unsuccessful. Analysis showed that no BF3 was removed by this technique. Methyl propionate is produced from ethylene and BF3.CH3OH.