반응 #94885

ord-0ab5300d0b84435cbc39a577bf0c8ea9

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타This compound is prepared by essentially the same procedure
  2. 2
    기타The product is obtained as a colorless oil upon distillation in vacuo (0.3 mm.)

실험 절차

This compound is prepared by essentially the same procedure as described in Example 1 Step A except that the 2-diethylaminoethyl chloride hydrochloride of Example 1 Step A is replaced by an equimolecular quantity of 3-dimethylamino-2-methylpropyl chloride hydrochloride. The product is obtained as a colorless oil upon distillation in vacuo (0.3 mm.).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04342782uspto-grants-1982_08