반응 #94706

반응 방정식

hydroquinone

sulfopropionic anhydride

2-hydroxypropyl methacrylate

monomethyl ether

→

METHACRYLOXYISOPROPYL SULFOPROPIONATE

용매

toluene

반응 조건

후처리

1. 1
   기타To a reaction vessel fitted with an air-bleed tube
2. 2
   기타sparged
3. 3
   건조with dry air as in (1) above
4. 4
   온도heated
5. 5
   workup.ADDITIONAfter 0.5 hour at 60° C. a solution containing 29% by weight of methacryloxyisopropyl sulfopropionate
6. 6
   기타is obtained

실험 절차

To a reaction vessel fitted with an air-bleed tube, thermometer, stirrer, and condenser there are charged sulfopropionic anhydride (29.1 g.), 2-hydroxypropyl methacrylate (29.1 g.), the monomethyl ether of hydroquinone (0.1 g.) and toluene (60 g.). The mixture is stirred, sparged with dry air as in (1) above and heated. After 0.5 hour at 60° C. a solution containing 29% by weight of methacryloxyisopropyl sulfopropionate is obtained.

출처