반응 #94592

반응 방정식

N2 (2-phenoxathiinylsulfonyl)-L-arginine

thionyl chloride

diethyl ether

→

N2 (2-phenoxathiinylsulfonyl)-L-arginyl chloride hydrochloride

반응 조건

후처리

1. 1
   기타resulted in a precipitate which
2. 2
   여과was collected by filtration
3. 3
   세척washed several times with dry diethyl ether

실험 절차

A suspension of 3 g of N2 -(2-phenoxathiinylsulfonyl)-L-arginine in 20 ml of thionyl chloride was stirred for 2 hours at room temperature. Addition of cold dry diethyl ether resulted in a precipitate which was collected by filtration and washed several times with dry diethyl ether to give N2 -(2-phenoxathiinylsulfonyl)-L-arginyl chloride hydrochloride.

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