반응 #9459

반응 방정식

4—Chloro-3-nitro-7-phenylquinoline

3-methylsulfanyl-propylamine

→

(3-methylsulfanylpropyl)-(3-nitro-7-phenylquinolin-4-yl)amine

수율 93.3%

반응 조건

후처리

1. 1
   workup.ADDITIONtreated
2. 2
   기타Recrystallization from isopropanol

실험 절차

4—Chloro-3-nitro-7-phenylquinoline (5.3 g, 18.8 mmol) and 3-methylsulfanyl-propylamine (2.17 g, 20.6 mmol) were combined and treated according to the general procedure described in Part E of Example 1. Recrystallization from isopropanol afforded 6.2 g of (3-methylsulfanylpropyl)-(3-nitro-7-phenylquinolin-4-yl)amine as gold plates.

출처