반응 #94477

ord-b2fa65e9bc3f4d82a1a83fb7c6b103df

반응 방정식

N=C(N)c1cccc([N+](=O)[O-])c1
3-nitrobenzamidine
O=[N+]([O-])c1ccc(C=CS(=O)(=O)Cl)cc1
4-nitrostyrylsulfonyl chloride
→
N=C(NS(=O)(=O)C=Cc1ccc([N+](=O)[O-])cc1)c1cccc([N+](=O)[O-])c1
N-(4-NITROSTYRYLSULFONYL)-3-NITROBENZAMIDINE

반응물

N=C(N)c1cccc([N+](=O)[O-])c1
3-nitrobenzamidine
O=[N+]([O-])c1ccc(C=CS(=O)(=O)Cl)cc1
4-nitrostyrylsulfonyl chloride

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Reaction of 3-nitrobenzamidine with 4-nitrostyrylsulfonyl chloride according to the above procedure provides N-(4-NITROSTYRYLSULFONYL)-3-NITROBENZAMIDINE, m.p. 230°-232° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04130663uspto-grants-1978_12