반응 #94458
ord-40b8cd088f1640418279c0a064ef507d
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
1,4-Diphenoxy-n-butane (24.2 g) and benzoyl chloride (29 g) are reacted in 250 ml of 1,2-dichloroethane in the presence of aluminum chloride (28 g) for 4 hours at 60° to yield 18.3 g (41% of theory) of colorless crystals mp 163°-4°. Calculated for C30H26O4 : C, 79.98% H, 5.82%. Found: C, 80.16%; H, 5.98%.