반응 #944006

ord-2aebb45d1c4140a6b49f0659aa90cf3d

반응 방정식

CS(=O)(=O)c1ccc(NC(C#N)c2ccc(OC(F)F)cc2)cc1
α-(4-difluoromethoxyphenyl)-α-(4-methylsulfonylanilino)acetonitrile
C/C=C/C=O
crotonaldehyde
CSc1ccc(NC(C#N)c2ccc(OC(F)F)cc2)cc1
title compound
CSc1ccc(NC(C#N)c2ccc(OC(F)F)cc2)cc1
α-(4-Difluoromethoxyphenyl)-α-(4-methylthioanilino)acetonitrile

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Following a procedure similar to that described in Example 1(iii), but using α-(4-difluoromethoxyphenyl)-α-(4-methylsulfonylanilino)acetonitrile [prepared as described in step (ii) above] and crotonaldehyde as starting materials, the title compound was obtained as a white powder (yield 31%), melting at 98-99° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: USRE039420E1uspto-grants-2006_12