반응 #943999

ord-e8566af10da04d4cb67722f52d006b8e

반응 방정식

CSc1ccc(NC(C#N)c2ccc(Cl)cc2)cc1
α-(4-chlorophenyl)-α-(4-methylthioanilino)acetonitrile
C=CC=O
acrolein
CSc1ccc(N=Cc2ccc(Cl)cc2)cc1
title compound
CSc1ccc(N=Cc2ccc(Cl)cc2)cc1
N-(4-Chlorobenzylidene)-4-methylthioaniline

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Following a procedure similar to that described in Example 21(iii), but using α-(4-chlorophenyl)-α-(4-methylthioanilino)acetonitrile [prepared as described in step (ii) above] and acrolein as starting materials, the title compound was obtained as an orange-colored powder (yield 32%), melting at 203-205° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: USRE039420E1uspto-grants-2006_12