반응 #943995

ord-fcbdbaec14734beb8ea06418f985b35f

반응 방정식

Cc1ccc(C(C#N)Nc2ccc(S(N)(=O)=O)cc2)cc1
α-(4-methylphenyl)-α-(4-sulfamoylanilino)acetonitrile
C=CC=O
acrolein
Cc1ccc(-c2cccn2-c2ccc(S(N)(=O)=O)cc2)cc1
title compound
Cc1ccc(-c2cccn2-c2ccc(S(N)(=O)=O)cc2)cc1
2-(4-Methylphenyl)-1-(4-sulfamoylphenyl)pyrrole

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Following a procedure similar to that described in Example 1(iii), but using α-(4-methylphenyl)-α-(4-sulfamoylanilino)acetonitrile [prepared as described in step (ii) above] and acrolein as starting materials, the title compound was obtained as a brown powder (yield 13%), melting at 183-184° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: USRE039420E1uspto-grants-2006_12