반응 #943992

반응 방정식

4-methylsulfonylbenzaldehyde

4-methoxyaniline

→

title compound

수율 95.0%

4-Methoxy-N-(4-methylsulfonylbenzylidene)aniline

수율 95.0%

용매

ethanol

반응 조건

후처리

1. 1
   온도the solution was heated
2. 2
   온도under reflux for 1 hour
3. 3
   기타the crystals which precipitated
4. 4
   여과were collected by filtration
5. 5
   세척washed with ethanol

실험 절차

1.00 g (5.4 mmol) of 4-methylsulfonylbenzaldehyde and 0.67 g (5.4 mmol) of 4-methoxyaniline were dissolved in 15 ml of ethanol, and the solution was heated under reflux for 1 hour. At the end of this time, the reaction solution was cooled to room temperature, and the crystals which precipitated were collected by filtration and washed with ethanol, to give 1.48 g (yield 95%) of the title compound as slightly yellow prismatic crystals.

출처