반응 #939024

ord-d59419bd63c8448a8bb5968fd6619d97

반응 방정식

CCOCCCl
2-chloroethyl ethyl ether
Cc1nc2ccccc2[nH]1
2-methylbenzimidazole
CCOCCn1c(C)nc2ccccc21
1-(2-Ethoxyethyl)-2-methyl-1H-benzimidazole
수율 82.0%

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

1-(2-Ethoxyethyl)-2-methyl-1H-benzimidazole was synthesized as in Synthesis Example 1 except that an equimolar amount of 2-methylbenzimidazole was used instead of benzimidazole, and an equimolar amount of 2-chloroethyl ethyl ether was used instead of 2-chloroethyl methyl ether. Yield 82%.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07252925B2uspto-grants-2007_08