반응 #939021
ord-7e233837b41f4ef9a3784255f4e715dd
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1온도was refluxed for 2 days
- 2기타water removed from the reaction mixture
- 3기타After reaction
- 4기타solvent was removed in vacuuo
- 5기타to yield a viscous oil
실험 절차
A mixture of 1,2,3-propanetricarboxylic acid (25 g), cyclohexanol (55 g), and p-toluenesulfonic acid (100 mg) in toluene (500 mL) was refluxed for 2 days and water removed from the reaction mixture. After reaction was complete, solvent was removed in vacuuo to yield a viscous oil. The crude material was redissolved in heptane and passed through a pad of silica gel to obtain 1,2,3-propanetricarboxylic acid tricyclohexyl ester (50 g) as a pale yellow oil.