반응 #939017

반응 방정식

mono-perphthalic acid

mono-perphthalic acid

sodium sulfite

→

2-Butylsulfonylcyclopentanone

용매

ether

반응 조건

후처리

1. 1
   세척the resultant solution was washed
2. 2
   기타evaporated
3. 3
   기타to remove the solvent
4. 4
   workup.DISTILLATIONdistilled

실험 절차

2-Buthylthiocyclopentanone (88 g) was reacted with a 30% excess solution of mono-perphthalic acid in ether at 0° C. After the reaction was completed, the excess mono-perphthalic acid was treated with sodium sulfite, and the resultant solution was washed, evaporated to remove the solvent, and then distilled, thereby giving 2-butylsulfonylcyclopentanone (78 g).

출처