반응 #93768

반응 방정식

Sodium 3,3-dimethyl-2-hydroxybutyrate

sodium hypochlorite

→

sodium 3,3-dimethyl-2-oxobutyrate

용매

water

반응 조건

후처리

1. 1
   workup.ADDITIONis slowly added

실험 절차

Sodium 3,3-dimethyl-2-hydroxybutyrate and ruthenium dioxide hydrate are added to water, the pH rendered alkaline, and sodium hypochlorite is slowly added to produce sodium 3,3-dimethyl-2-oxobutyrate in high yield and purity. The solid catalyst is filtered off and may be re-used while the filtrate can be directly used in further synthesis.

출처