반응 #936319

ord-151e9ce2491f49758603e3ddba6e4ef6

반응 방정식

COC1=NC(Cc2ccccc2)CCC=C1
product
COC1=NC(Cc2ccccc2)CCC=C1
3,4-dihydro-7-methoxy-2-(phenylmethyl)-2H-azepine
[Cl-].[NH4+]
ammonium chloride
→
Cl.N=C1C=CCCC(Cc2ccccc2)N1
title compound
Cl.N=C1C=CCCC(Cc2ccccc2)N1
1,5,6,7-tetrahydro-7-(phenylmethyl)-2H-azepin-2-imine, monohydrochloride

반응물

COC1=NC(Cc2ccccc2)CCC=C1
product
COC1=NC(Cc2ccccc2)CCC=C1
3,4-dihydro-7-methoxy-2-(phenylmethyl)-2H-azepine
[Cl-].[NH4+]
ammonium chloride

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

The product of Example 188 is reacted with ammonium chloride by the method of Example 5 to generate the title compound.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06011028uspto-grants-2000_01