반응 #9346
ord-ec11d9e4f3f449f6a915145c8ea66bec
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타The resulting waxy solid was purified by chromatography on silica gel
실험 절차
Sodium propanoate (0.88 g, 1.5 eq) and 2,6-dipropylphenol (1.09 g, 1.0 eq) were combined in Triflic Acid (5.0 g) as in Example 13, step 1. The resulting waxy solid was purified by chromatography on silica gel using ethyl acetate:hexanes:acetic acid (10:90:1) to give the titled phenol.