반응 #9230

반응 방정식

1-(6-bromo-2-benzothiazolyl)-3-ethylurea

dppp

triethylamine

styrene

→

desired compound

수율 62.0%

1-(6-(2(E)-Phenylvinyl)-2-benzothiazolyl)-3-ethylurea

수율 62.0%

용매

DMF

반응 조건

후처리

1. 1
   기타was reacted

실험 절차

A mixture of 1-(6-bromo-2-benzothiazolyl)-3-ethylurea, Pd(PPh3)2Cl2, dppp, triethylamine, styrene, and two crystals of BHT in anhydrous DMF was reacted according to the procedure of Example 225 to give the desired compound 0.201 g (62%). LC/MS 324.2 (M+1); LC retention time 2.87 min.

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