반응 #9226

반응 방정식

1-(6-bromo-2-benzothiazolyl)-3-ethylurea

triethylamine

phenylacetylene

→

desired compound

수율 8.0%

1-(6-Phenylacetylenyl-2-benzothiazolyl)-3-ethylurea

수율 8.0%

용매

DMF

반응 조건

후처리

1. 1
   기타was reacted

실험 절차

A mixture of 1-(6-bromo-2-benzothiazolyl)-3-ethylurea, Pd(PPh3)2Cl2, triethylamine, and phenylacetylene in 1 mL of anhydrous DMF was reacted according to the procedure of Example 213 to give 0.008 g (8%) of the desired compound. LC/MS 322 (M+1); LC retention time 3.65 min.

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