반응 #9108

반응 방정식

acetyl chloride

dimethylamine

2-methylbenzaldehyde

→

dimethyl-(2-methyl-benzylidene)-ammonium chloride

반응 조건

후처리

1. 1
   기타with general synthesis instructions 3

실험 절차

The reaction of 14.0 ml (0.108 mol) dimethylamine solution and 4.6 ml (0.040 mol) 2-methylbenzaldehyde in accordance with general synthesis instructions 1 and subsequent reaction with 2.4 ml (0.040 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 5.3 g (corresponding to 73% of the yield calculated by theory) dimethyl-(2-methyl-benzylidene)-ammonium chloride.

출처