반응 #9105
ord-00adf1ba992d4cb99f816842b438f344
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타with general synthesis instructions 3
실험 절차
The reaction of 9.5 ml (0.096 mol) piperidine and 4.7 ml (0.040 mol) 2-methylbenzaldehyde in accordance with general synthesis instructions 2 and subsequent reaction with 2.4 ml (0.040 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 5.8 g (corresponding to 65% of the yield calculated by theory) 1-(2-methyl-benzylidene)-piperidinium chloride.