반응 #91042

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3-bromopentane

2-chloro-3-ethoxy-5-iodophenol

2-Chloro-3-ethoxy-5-iodophenol

→

2-Chloro-1-ethoxy-5-iodo-3-(pentan-3-yloxy)benzene

수율 79.0%

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실험 절차

2-Chloro-1-ethoxy-5-iodo-3-(pentan-3-yloxy)benzene (8) (1.2 g, 79%) was prepared from 2-chloro-3-ethoxy-5-iodophenol (7) (1.1 g, 3.7 mmol) using a procedure essentially the same as in step (i) for AAA-001 except that 3-bromopentane was used instead of cyclopentyl bromide.

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