반응 #9097

반응 방정식

acetyl chloride

pyrrolidine

2-methylbenzaldehyde

→

1-(2-methyl-benzylidene)-pyrrolidinium chloride

반응 조건

후처리

1. 1
   기타with general synthesis instructions 3

실험 절차

The reaction of 8.2 ml (0.100 mol) pyrrolidine and 7.0 g (0.050 mol) 2-methylbenzaldehyde in accordance with general synthesis instructions 2 and subsequent reaction with 3.9 g (0.050 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 6.6 g (corresponding to 63% of the yield calculated by theory) 1-(2-methyl-benzylidene)-pyrrolidinium chloride.

출처