반응 #89137

ord-8331ed1e45e9497ab8994b075d440a51

반응 방정식

O=CC1=CCCC1
cyclopenten-1-aldehyde
CCOC(=O)C(NC(C)=O)C(=O)OCC
diethyl acetamidomalonate
→
CCOC(=O)C1(C(=O)OCC)C2CCCC2CN1C(C)=O
title compound
CCOC(=O)C1(C(=O)OCC)C2CCCC2CN1C(C)=O
rac-Diethyl 2-acetylhexahydrocyclopenta[c]pyrrole-1,1(2H)-dicarboxylate

반응물

O=CC1=CCCC1
cyclopenten-1-aldehyde
CCOC(=O)C(NC(C)=O)C(=O)OCC
diethyl acetamidomalonate

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

The title compound was prepared from cyclopenten-1-aldehyde (1 eq) and diethyl acetamidomalonate (1 eq) using the procedure by Chung et al. (J. Org. Chem. 1990, 55, 270). MS (ESI) 298 (M+H)

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US09440982B2uspto-grants-2016_09